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Vacuum Evaporator
Evaporation, Concentration & Solvent Recovery

Vacuum Evaporator

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Stainless-steel agitated process vessel with a motor and gearbox drive, open manways, a vapour pipe and a condenser line in an installed plant

Vacuum Evaporator

A vacuum evaporator is the practical starting point for a processor who needs to concentrate a heat-sensitive liquid in modest, changing batches: botanical extracts, fruit or flavour concentrates, and pharmaceutical or nutraceutical liquids. It is a single jacketed, agitated vessel run under reduced pressure, so the liquid boils at a lower temperature than it would in the open. Four things need to be decided before it can be sized: the batch volume and how many batches a day, the solids in the feed and the final solids or Brix wanted, how much heat the product can take, and which heat source and vacuum utility the site can support. It is not a continuous or high-capacity machine; where volumes are large, where the liquid fouls heavily or where steam economy dominates, a film, forced-circulation or multiple-effect arrangement is the better fit. The evaporator is listed as a complete vessel, condenser, vacuum and control package for such batch duties.

Feed is loaded into a jacketed vessel with an agitator. The vacuum system lowers the pressure to the chosen set point, so the liquid boils at a correspondingly lower temperature, while steam, hot water or thermic fluid in the jacket supplies gentle heat. The agitator keeps the batch moving against the heated wall, which helps limit burn-on and uneven concentration; Boiling under vacuum at about 60-70 °C, depending on the degree of vacuum, gives fruit products better taste and flavour retention. Vapour leaves through a demister to a condenser and is collected as condensate. The batch is held under vacuum and agitation until density, refractometer or temperature readings show that the target concentration or solids has been reached. Because a single vessel has no fixed film or circulation geometry, changing from one product to the next is simple and cleaning in place between batches is straightforward, which suits multi-product work and trial programmes. The price of that flexibility is running cost: a batch vessel makes no attempt to reuse vapour heat, so energy use per kilogram of water removed is higher than in a multi-effect train, which passes vapour heat from stage to stage. The vessel, jacket, agitator and vacuum equipment are in SS 316L or another suitable grade, with CIP connections and PLC-based instrumentation. Volume and vacuum rating follow the batch size and the product.

Key Specification Inputs

Feed solids, final Brix, product sensitivity and energy.

Process Flow

Vacuum Evaporator process flow — batch charging, vacuum drawdown, jacketed heating and agitation, controlled boiling and evaporation, vapour extraction and condensation, endpoint monitoring, batch discharge, CIP and changeover

Technical Specifications

Evaporator TypeVacuum evaporator: a general-purpose agitated vessel
Working PrincipleLower vessel pressure reduces the boiling point, so the batch is concentrated at low temperature with gentle jacket heat
VesselJacketed and agitated, for batch or semi-continuous operation
AgitationMotor-driven agitator; type and speed matched to product viscosity
Heating MediumSteam, hot water or thermic fluid in the jacket, as configured
Operating ModeUnder vacuum, for low-temperature concentration of heat-sensitive product
Suitable DutyGeneral batch concentration of smaller volumes, with frequent product changes
Contact MaterialSS 316L, or another grade suited to the product
Condensing SystemSurface or barometric condenser with vacuum ejector or pump
AutomationPLC control of temperature, vacuum and batch endpoint; SCADA can be configured
CleaningProduct-contact circuit arranged for clean-in-place
Batch FlexibilityHandles different products and varying batch sizes in the same vessel
CapacitySized to the requirement, from pilot scale to mid-scale batch duty
UtilitiesSteam, hot water or thermic fluid for the jacket; cooling water, vacuum utilities, electric power and compressed air

Plant Capacities

ScaleTypical Batch SizeVessel ConfigurationTypical Duty
Pilot / R&DSmall batchSingle jacketed agitated vesselFormulation and process development
Small commercialMid-size batchSized jacketed vessel with agitatorGeneral batch concentration, flexible product mix
Mid-scale commercialLarger batch or semi-continuousLarger jacketed vessel, upgraded vacuum systemHigher-volume general-purpose evaporation

Vessel volume, agitator duty and vacuum system follow from the batch size, product viscosity and heat sensitivity. For continuous, high-throughput or strongly fouling duty, a film, forced-circulation or multi-effect evaporator is normally the better fit.

Typical Process Route

1

Define Batch, Solids and Endpoint

Batch volume, feed solids, final Brix or solids, heat limits and the cleaning routine between products are fixed first, since they set vessel size, jacket area and vacuum capacity.

2

Loading the Vessel

The feed goes into the jacketed, agitated vessel, either as a single charge or in stages when the operation is run semi-continuously.

3

Drawing the Vacuum

The vacuum system takes the vessel down to the operating pressure, which lowers the temperature at which the liquid will boil before heating starts.

4

Heating and Mixing

Steam, hot water or thermic fluid flows through the jacket and the agitator keeps the batch moving, spreading heat evenly and limiting burn-on at the wall.

5

Gentle Boiling

The batch boils at the lowered temperature, releasing water or solvent while stirring keeps the concentration uniform.

6

Removing and Condensing Vapour

Vapour is pulled off through a demister to the condenser and collected as condensate, which may be reused or disposed of according to its quality.

7

Watching the Endpoint

Density, refractometer or temperature-rise instruments follow the batch towards the target concentration, moisture or solids.

8

Discharging the Batch

At the endpoint the concentrate leaves through the bottom valve to storage or to the next stage, for example drying.

9

Cleaning and Changeover

Vessel, jacket and agitator are cleaned in place between batches or products, so one unit can serve several products. Low-temperature vacuum evaporation can let bacteria multiply in the equipment, so cleaning is frequent and a sanitising step is planned.

Major Plant Equipment

  • Jacketed, agitated evaporator vessel
  • Agitator motor and gearbox
  • Jacket supply for steam, hot water or thermic fluid
  • Vapour outlet with demister
  • Surface or barometric condenser
  • Vacuum system, using a steam ejector or liquid-ring pump
  • Condensate receiver and pump
  • Bottom discharge valve and pump
  • Density or refractometer and temperature instruments
  • CIP skid with spray-ball connections
  • Temperature and vacuum or pressure transmitters
  • PLC control panel with motor control centre

Plant Output

Concentrated batch productCondensate from the recovered vapour

Applications

  • Batch concentration of pharmaceutical and nutraceutical liquids
  • Low-temperature pre-concentration of heat-sensitive extracts
  • Small and medium batches of food and flavour concentrates
  • Contract work with frequent product changes
  • Trial and pilot concentration before scale-up
  • Recovering solvent from small-volume process residues
  • Pre-concentrating botanical extracts before drying or crystallisation
  • Thickening viscous formulations under vacuum

Key Features

  • One Vessel, Many Products

    A single agitated, vacuum-rated vessel takes varied batch sizes and product changes without the fixed geometry of a film or forced-circulation body.

  • Low-Temperature Concentration

    Operating under vacuum lowers the boiling point, so heat-sensitive liquids avoid the thermal stress of boiling at atmospheric pressure.

  • Even Heating through Agitation

    Stirring continuously moves liquid across the jacketed wall, which helps limit burn-on and gives a more uniform concentration.

  • Simple Cleaning and Changeover

    A single vessel with clean-in-place connections makes switching between products quick and repeatable.

  • Sized for Small and Pilot Duty

    It fits smaller batches and development programmes, and a move to a film, forced-circulation or multi-effect unit is possible as volumes grow.

Frequently Asked Questions

Who is a vacuum evaporator for, and what should be settled first?
Processors concentrating heat-sensitive liquids in batches of changing size. Settle the batch volume and batches per day, feed solids and final Brix, the temperature the product tolerates, the heat source and cooling water available, and how the vacuum will be produced. These inputs decide vessel size and jacket area.
How does it work?
A vacuum pump or ejector lowers the pressure in a jacketed, agitated vessel so the liquid boils at a lower temperature. The jacket heats gently, the agitator mixes, and the vapour passes to a condenser. The batch is held until the chosen concentration is reached.
How does it differ from a falling-film or multiple-effect evaporator?
It is a single batch vessel, whereas a falling-film evaporator or an MEE multiple effect evaporator uses dedicated tube or multi-vessel arrangements for continuous, larger or fouling duties. The vacuum evaporator gives flexibility; the others give throughput and lower steam use per unit of water removed.
What does running it cost in energy?
Steam or other jacket heat and cooling water are the main items, plus power for the vacuum system and agitator. Because the vapour is not reused, the heat demand per kilogram of water removed is higher than in multi-effect designs, where each stage heats the next. For modest batch volumes this is often acceptable; for larger continuous volumes it usually is not.
Which products suit it?
Heat-sensitive liquids in smaller or varied batches: pharmaceutical and nutraceutical liquids, botanical extract pre-concentration, and flavour or food concentrates, especially where one vessel must serve several products. Small vacuum evaporators suit medium-size operations in developing countries, and a stirred vacuum evaporator is one way to concentrate fruit purée, apricot up to 28 Brix. Foaming or heavily fouling feeds need a closer look before this type is chosen.
Can it be used for trials before a larger plant is built?
Yes. A batch vessel is a practical way to test concentration on your own feed, and to find out how the product behaves with respect to foaming, fouling and final viscosity. The results then guide the choice of a continuous plant, and concentrate can be taken on to a spray dryer if powder is the aim.
How should a feed be prepared in a warm climate?
Filter or screen it to remove solids, keep feed tanks clean and avoid long holds at ambient temperature. Because bacteria can multiply in low-temperature vacuum evaporators, frequent stops to sanitise the equipment are advised, and chilled or prompt handling of perishable feeds is the safer course.
What should be prepared for a technical proposal?
Feed composition, solids and viscosity, final Brix or solids, heat sensitivity, batch size and number of batches, available heat source, cooling water and power, and the cleaning routine between products. A trial on the actual product is advised. Related plants are grouped under the evaporation and solvent recovery category, and juice duties under fruit juice processing.
What does the listed system include?
The vessel, agitator, condenser, vacuum system and automation, with installation and commissioning confirmed in the technical proposal. The vacuum source changes the utilities needed: a steam ejector draws motive steam and cooling water, while a liquid-ring pump draws electric power and seal water.

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